ChemicalBook CAS DataBase List CX6258

CX6258 synthesis

6synthesis methods

Product Name:CX6258
CAS Number:1202916-90-2
Molecular formula:C26H24ClN3O3
Molecular Weight:461.94

17630-75-0 Synthesis

17630-75-0
287 suppliers
$10.00/1g

1202916-90-2
96 suppliers
$39.00/1mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: piperidine / ethanol / 20 - 40 °C / Inert atmosphere
1.2: 2 h / 0 °C
2.1: hydrogenchloride / water / 0.5 h / 20 °C
3.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
3.2: 24 h / 20 °C / Inert atmosphere

References:

Haddach, Mustapha;Michaux, Jerome;Schwaebe, Michael K.;Pierre, Fabrice;O'Brien, Sean E.;Borsan, Cosmin;Tran, Joe;Raffaele, Nicholas;Ravula, Suchitra;Drygin, Denis;Siddiqui-Jain, Adam;Darjania, Levan;Stansfield, Ryan;Proffitt, Chris;MacAlino, Diwata;Streiner, Nicole;Bliesath, Joshua;Omori, May;Whitten, Jeffrey P.;Anderes, Kenna;Rice, William G.;Ryckman, David M. [ACS Medicinal Chemistry Letters,2012,vol. 3,# 2,p. 135 - 139]

4318-37-0 Synthesis