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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
58648-13-8

Cyclohexanone, 2-acetyl-2-methyl-, (-)- synthesis

10synthesis methods
Cyclohexene, 1-methyl-2-[(trimethylsilyl)oxy]-

19980-35-9
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75-36-5 Synthesis
Acetyl chloride

75-36-5
579 suppliers
$17.92/100G

Cyclohexanone, 2-acetyl-2-methyl-, (-)-

58648-13-8
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Yield:58648-13-8 91%

Reaction Conditions:

with titanium tetrachloride in dichloromethane at -78; for 1 h;-78 deg C up to room temp within 2 h;

References:

Fleming;Iqbal;Krebs [Tetrahedron,1983,vol. 39,# 6,p. 841 - 846]

874-23-7 Synthesis
2-ACETYLCYCLOHEXANONE

874-23-7
232 suppliers
$8.00/1g

Iodomethane

74-88-4
350 suppliers
$15.00/10g

Cyclohexanone, 2-acetyl-2-methyl-, (-)-

58648-13-8
2 suppliers
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References
7-Octene-2,4-dione, 3-methyl-

15867-49-9
0 suppliers
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Cyclohexanone, 2-acetyl-2-methyl-, (-)-

58648-13-8
2 suppliers
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References
ACETYL FLUORIDE

557-99-3
27 suppliers
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Cyclohexene, 1-methyl-2-[(trimethylsilyl)oxy]-

19980-35-9
0 suppliers
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Cyclohexanone, 2-acetyl-2-methyl-, (-)-

58648-13-8
2 suppliers
inquiry

References
1-Cyclohexen-1-ol, 2-methyl-, acetate

1196-73-2
0 suppliers
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Cyclohexanone, 2-acetyl-2-methyl-, (-)-

58648-13-8
2 suppliers
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References