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ChemicalBook CAS DataBase List CYCLOPENTYL-THIOUREA
102936-57-2

CYCLOPENTYL-THIOUREA synthesis

3synthesis methods
-

Yield: 85%

Reaction Conditions:

with ammonia in methanol at 20; for 20 h;

Steps:

1
Isothiocyanate (50 mmol) and ammonia (30 mL) were added to the reaction tube, stirred in methanol at room temperature for 20 hours, and the precipitated solid was recrystallized with ethyl acetate to obtain pure thiourea with a yield of 85%.

References:

UNIV CHANGZHOU;Changzhou University;LI JIAN;Li Jian;WEN JINXIA;Wen Jinxia;LIU LI;Liu Li CN111777604, 2020, A Location in patent:Paragraph 0026; 0028

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