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cyclopropane-1,1-diyldiMethanaMine synthesis

4synthesis methods
39590-81-3 Synthesis
1,1-Bis(hydroxymethyl)cyclopropane

39590-81-3
284 suppliers
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cyclopropane-1,1-diyldiMethanaMine

38932-70-6
6 suppliers
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 76 percent / pyridine / 2 h / 0 - 5 °C
2: 93 percent / NaN3 / dimethylsulfoxide / 16 h / 58 - 65 °C
3: Ph3P / tetrahydrofuran; H2O / 15 h

References:

Wade, Peter A.;Kondracki, Paul A.;Carroll, Patrick J. [Journal of the American Chemical Society,1991,vol. 113,# 23,p. 8807 - 8811]

136476-38-5 Synthesis
1,1-CyclopropanediMethanol diMethanesulfonate

136476-38-5
11 suppliers
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cyclopropane-1,1-diyldiMethanaMine

38932-70-6
6 suppliers
inquiry