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ChemicalBook CAS DataBase List Cyclopropanecarboxaldehyde

Cyclopropanecarboxaldehyde synthesis

9synthesis methods
Cyclopropanecarboxaldehyde is prepared by reaction of cyclopropylmethanol. The reaction needs reagent pyridinium chlorochromate and solvent CH2Cl2 with other condition of ambient temperature for 3 hours. The yield is about 60%.
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Yield:1489-69-6 91.2%

Steps:

3 Isomerization of DHF to CPCA

After an additional distillation for recovery of remaining DHF, crude CPCA was obtained which analyzed as follows: 91.2% CPCA, 5.7% crotonaldehyde, and 0.5% tetrahydrofuran.

References:

US4275238,1981,A

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