DIETHYL 2,4,6-TRIMETHYLPHENYL MALONATE synthesis
- Product Name:DIETHYL 2,4,6-TRIMETHYLPHENYL MALONATE
- CAS Number:94430-86-1
- Molecular formula:C16H22O4
- Molecular Weight:278.34
Yield:94430-86-1 57%
Reaction Conditions:
Stage #1: diethyl malonatewith sodium hydride in 1-methyl-pyrrolidin-2-one at 0 - 20;Inert atmosphere;
Stage #2: iodomesitylenewith copper(l) iodide in 1-methyl-pyrrolidin-2-one at 80 - 85; for 5 h;Inert atmosphere;
References:
Muehlebach, Michel;Boeger, Manfred;Cederbaum, Fredrik;Cornes, Derek;Friedmann, Adrian A.;Glock, Jutta;Niderman, Thierry;Stoller, Andre;Wagner, Trixie [Bioorganic and Medicinal Chemistry,2009,vol. 17,# 12,p. 4241 - 4256] Location in patent:experimental part
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