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ChemicalBook CAS DataBase List DifluoroiodoMethyl phenyl sulfone
802919-90-0

DifluoroiodoMethyl phenyl sulfone synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
2.1: copper(l) iodide; cesium fluoride / N,N-dimethyl-formamide / 4 h / -30 °C
2.2: 16 h / 0 °C / In air

References:

Zhu, Jieming;Wang, Fei;Huang, Weizhou;Zhao, Yanchuan;Ye, Wenchao;Hu, Jinbo [Synlett,2011,# 7,p. 899 - 902]