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ChemicalBook CAS DataBase List Dimethenamid

Dimethenamid synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sodium acetate; acetic anhydride / 7 h / 120 °C / Inert atmosphere
1.2: 30 °C / pH 7 - 8
2.1: hydroxylamine hydrochloride / methanol / 7 h / Reflux
3.1: toluene-4-sulfonic acid / cyclohexane
3.2: ligand-containing iridium catalyst / 20 °C

References:

Beijing Yingtaijiahe Biological Technology Co., Ltd.;Wu Hao;Huang Guangying;Yang Haijian CN110066268, 2019, A

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