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Dimethylcyclohexanone-2,6-dicarboxylate synthesis

2synthesis methods
-

Yield: 32%

Reaction Conditions:

with poly(dimethylsiloxane-co-methylhydrosiloxane)trimethylsilyl terminated supported 1-carboxy-6-ethyl-1,8-diazabicyclo[5.4.0]undec-7-ene in methanol at 25 - 27; under 760.051 Torr; for 4 h;

References:

Beckman, Eric J.;Munshi, Pradip [Green Chemistry,2011,vol. 13,# 2,p. 376 - 383] Location in patent:experimental part