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ChemicalBook CAS DataBase List DIPYRIDIN-3-YLMETHANE
78210-43-2

DIPYRIDIN-3-YLMETHANE synthesis

5synthesis methods
35779-35-2 Synthesis
DIPYRIDIN-3-YLMETHANONE

35779-35-2
46 suppliers
$45.00/10mg

-

Yield:78210-43-2 96%

Reaction Conditions:

Stage #1: di-3-pyridylmethanonewith potassium hydroxide in ethylene glycol at 20; for 1 h;Inert atmosphere;Wolff-Kishner reduction;
Stage #2: with hydrazine hydrate at 185; for 1.75 h;Inert atmosphere;Wolff-Kishner reduction;

References:

Park, Byung Sun;Lee, Sang Woo;Kim, In Tae;Tae, Jin Sung;Lee, So Ha [Heteroatom Chemistry,2012,vol. 23,# 1,p. 66 - 73] Location in patent:experimental part