Ethanone, 1-[2-(1-propynyl)phenyl]- (9CI) synthesis
3synthesis methods
- Product Name:Ethanone, 1-[2-(1-propynyl)phenyl]- (9CI)
- CAS Number:171258-00-7
- Molecular formula:C11H10O
- Molecular Weight:158.2
Yield:171258-00-7 92%
Reaction Conditions:
Stage #1: methyl iodidewith magnesium in diethyl ether at 20; for 0.333333 h;
Stage #2: 2-(prop-1-yn-1-yl)benzaldehyde in diethyl ether at 0; for 4 h;
References:
Nishida, Masaki;Lee, Donghyeon;Shintani, Ryo [Journal of Organic Chemistry,2020,vol. 85,# 13,p. 8489 - 8500]