ethyl 2-(1H-inden-2-yl)acetate synthesis
- Product Name:ethyl 2-(1H-inden-2-yl)acetate
- CAS Number:96437-60-4
- Molecular formula:C13H14O2
- Molecular Weight:202.25
Yield:96437-60-4 49.5%
Reaction Conditions:
Stage #1: diethoxyphosphoryl-acetic acid ethyl esterwith sodium hydride in tetrahydrofuran at 10 - 20; for 1.5 h;
Stage #2: 2-indanone in tetrahydrofuran at 0 - 20; for 1.5 h;
Stage #3: with water at 20;
References:
US6339135,2002,B1 Location in patent:Page column 23
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