ETHYL-4-(4-CYANOPHENYL)-4-OXOBUTYRATE synthesis
- Product Name:ETHYL-4-(4-CYANOPHENYL)-4-OXOBUTYRATE
- CAS Number:25370-40-5
- Molecular formula:C13H13NO3
- Molecular Weight:231.25
623-73-4
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Yield:25370-40-5 89%
Reaction Conditions:
with tert.-butylhydroperoxide;[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-κN1,κN1′]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC]iridium hexafluorophosphate;1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile at 20; for 15 h;Sealed tube;Irradiation;Inert atmosphere;
References:
Li, Fang;Zhu, Siqi;Koenigs, Rene M. [Chemical Communications,2022,vol. 58,# 54,p. 7526 - 7529] Location in patent:supporting information