ETHYL MESITYLGLYOXYLATE synthesis
- Product Name:ETHYL MESITYLGLYOXYLATE
- CAS Number:5524-57-2
- Molecular formula:C13H16O3
- Molecular Weight:220.26
1667-04-5
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4755-77-5
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5524-57-2
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Yield:5524-57-2 99%
Reaction Conditions:
Stage #1: 2-bromomesitylenewith lithium in diethyl ether at 20; for 3 h;
Stage #2: with copper(l) cyanide in tetrahydrofuran;diethyl ether at -65 - -60; for 1.5 h;Cooling with acetone-dry ice;
Stage #3: Ethyl oxalyl chloride in tetrahydrofuran;diethyl ether at -60 - 20;
References:
Screttas, Constantinos G.;Steele, Barry R.;Micha-Screttas, Maria;Heropoulos, Georgios A. [Organic Letters,2012,vol. 14,# 22,p. 5680 - 5683] Location in patent:supporting information
4755-77-5
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108-67-8
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5524-57-2
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57386-83-1
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$60.00/100mg
4755-77-5
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1407160-10-4
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5524-57-2
29 suppliers
$31.80/1gm:
