Formamide, N-(2-phenylethyl)- synthesis
- Product Name:Formamide, N-(2-phenylethyl)-
- CAS Number:23069-99-0
- Molecular formula:C9H11NO
- Molecular Weight:149.19
Yield: 89%
Reaction Conditions:
with manganese(II) chloride tetrahydrate at 150; for 10 h;Inert atmosphere;Sealed tube;
Steps:
Control trials 1 to 9
General procedure: Phenethylamine (0.2 mmol),catalyst,Carboxamides (1.0 mL) were addedIn a 10 mL reaction vessel,Argon protection,Heating reaction,The product was quantitatively analyzed by 1H NMR;The specific reaction conditions for each control group are shown in Table 1.
References:
Xiangtan University;Gong Xing;Xie Guilin;Cai Changqun;Zhang Jingyu CN107986927, 2018, A Location in patent:Paragraph 0079; 0080; 0081; 0082; 0084
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