Formamide, N-(2-phenylethyl)- synthesis

11synthesis methods

Product Name:Formamide, N-(2-phenylethyl)-
CAS Number:23069-99-0
Molecular formula:C9H11NO
Molecular Weight:149.19

627-45-2 Synthesis

627-45-2
114 suppliers
$66.00/25mL

64-04-0
8 suppliers
$10.00/5mL

23069-99-0
27 suppliers
$56.20/1g

Yield: 89%

Reaction Conditions:

with manganese(II) chloride tetrahydrate at 150; for 10 h;Inert atmosphere;Sealed tube;

Steps:

Control trials 1 to 9
General procedure: Phenethylamine (0.2 mmol),catalyst,Carboxamides (1.0 mL) were addedIn a 10 mL reaction vessel,Argon protection,Heating reaction,The product was quantitatively analyzed by 1H NMR;The specific reaction conditions for each control group are shown in Table 1.

References:

Xiangtan University;Gong Xing;Xie Guilin;Cai Changqun;Zhang Jingyu CN107986927, 2018, A Location in patent:Paragraph 0079; 0080; 0081; 0082; 0084

64-18-6 Synthesis