ChemicalBook CAS DataBase List gossypolone

gossypolone synthesis

3synthesis methods

Product Name:gossypolone
CAS Number:4547-72-2
Molecular formula:C30H26O10
Molecular Weight:546.52

303-45-7 Synthesis

303-45-7
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4547-72-2
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Yield:4547-72-2 91%

Reaction Conditions:

Stage #1: (rac)-gossypolwith iron(III) chloride;acetic acid in water;acetone at 100; for 2 h;
Stage #2: with sulfuric acid in diethyl ether;water;

References:

Dodou, Kalliopi;Anderson, Rosaleen J.;Lough, W. John;Small, David A. P.;Shelley, Michael D.;Groundwater, Paul W. [Bioorganic and Medicinal Chemistry,2005,vol. 13,# 13,p. 4228 - 4237]

1189561-66-7
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4547-72-2
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References

[2,2'-Binaphthalene]-1,1',4,4'-tetrone, 8,8'-bis(1,3-dithian-2-yl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-5,5'-bis(1-methylethyl)-

609848-53-5
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4547-72-2
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References

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