ChemicalBook CAS DataBase List GW0742

GW0742 synthesis

10synthesis methods

Product Name:GW0742
CAS Number:317318-84-6
Molecular formula:C21H17F4NO3S2
Molecular Weight:471.49

933782-03-7 Synthesis

933782-03-7
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317318-84-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: thionyl chloride / chloroform / 5 h / 0 - 20 °C
2.1: caesium carbonate / acetonitrile / 2 h / 20 °C
2.2: 14 h / 20 °C
3.1: sodium carbonate / 1,2-dimethoxyethane / 0.5 h / 150 °C / Inert atmosphere; Sealed tube; Microwave irradiation
4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

References:

Teske, Kelly A.;Rai, Ganesha;Nandhikonda, Premchendar;Sidhu, Preetpal S.;Feleke, Belaynesh;Simeonov, Anton;Yasgar, Adam;Jadhav, Ajit;Maloney, David J.;Arnold, Leggy A. [ACS Combinatorial Science,2017,vol. 19,# 10,p. 646 - 656]

22900-83-0 Synthesis