HYDROCINCHONINE synthesis
- Product Name:HYDROCINCHONINE
- CAS Number:485-65-4
- Molecular formula:C19H24N2O
- Molecular Weight:296.41
491-35-0
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485-65-4
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: lithium diisopropylamide, pyridine hydrochloride
2: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature
3: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h
4: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min
5: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h
6: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h
References:
Brown, Richard T.;Curless, Dale [Tetrahedron Letters,1986,vol. 27,# 49,p. 6005 - 6008]
118-10-5
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485-65-4
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$65.40/10mg
109922-57-8
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485-65-4
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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485-65-4
57 suppliers
$65.40/10mg
1000210-73-0
0 suppliers
inquiry
485-65-4
57 suppliers
$65.40/10mg