ChemicalBook CAS DataBase List ISOPROPYLAMINE HYDROCHLORIDE

ISOPROPYLAMINE HYDROCHLORIDE synthesis

5synthesis methods

Product Name:ISOPROPYLAMINE HYDROCHLORIDE
CAS Number:15572-56-2
Molecular formula:C3H10ClN
Molecular Weight:95.57

75-31-0 Synthesis

75-31-0
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$14.00/25mL

15572-56-2
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$14.14/1gm:

Yield:15572-56-2 100%

Reaction Conditions:

with hydroxylamine hydrochloride in ethanol for 2 h;Reflux;

Steps:

General procedure for the preparation of amine hydrochloride salts 2c-2r
General procedure: To a 25-mL round-bottomed flask containing ammonium chloride (0.54 g, 10 mmol) was added ethanol (3 mL) followed by the requisite amine (10 mmol). The mixture was magnetically stirred and refluxed for 2 h. The solvent was then removed by rotary evaporation affording the hydrochloride salt as a solid invariably in quantitative yield.

References:

Di Grandi, Martin J.;Bennett, Caitlin;Cagino, Kristen;Muccini, Arnold;Suraci, Corey;Saba, Shahrokh [Synthetic Communications,2015,vol. 45,# 22,p. 2601 - 2607] Location in patent:supporting information

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