![](/CAS/GIF/503-74-2.gif)
Isovaleric acid synthesis
- Product Name:Isovaleric acid
- CAS Number:503-74-2
- Molecular formula:C5H10O2
- Molecular Weight:102.13
![Isovaleraldehyde](/CAS/GIF/590-86-3.gif)
590-86-3
355 suppliers
$10.00/5g
![Isovaleric acid](/CAS/GIF/503-74-2.gif)
503-74-2
401 suppliers
$5.00/10g
Yield:503-74-2 99.1%
Reaction Conditions:
with potassium acetate;palladium diacetate;C34H36O8 at 30 - 35; for 6 h;Catalytic behavior;Inert atmosphere;Reagent/catalyst;
Steps:
7-12 Example 7
General procedure: To a dry 1L three-neck flask, add isovaleraldehyde (160g, 1.86mol), isovaleric acid (160g, 1.57mol), the above ligand L2 (24.8mg, 0.04mmol), palladium acetate (44.9mg, 0.2mmol) ) And potassium acetate 260mg; mechanically stirred under a nitrogen atmosphere, after the temperature rises to 30°C, start to pass in air at a flow rate of 19.8g/h, and keep the reaction temperature between 3035°C by adding cooling water to the water bath Reaction in any range, after 8h reaction, isovaleric acid is prepared.
References:
CN110776412,2020,A Location in patent:Paragraph 0087-0111
![3-Methyl-1-butanol](/CAS/GIF/123-51-3.gif)
123-51-3
519 suppliers
$25.00/25mL
![Isovaleric acid](/CAS/GIF/503-74-2.gif)
503-74-2
401 suppliers
$5.00/10g
![Valeraldehyde](/CAS/GIF/110-62-3.gif)
110-62-3
240 suppliers
$13.44/25ML
![Isovaleraldehyde](/CAS/GIF/590-86-3.gif)
590-86-3
355 suppliers
$10.00/5g
![Isovaleric acid](/CAS/GIF/503-74-2.gif)
503-74-2
401 suppliers
$5.00/10g
![Valeric acid](/CAS/GIF/109-52-4.gif)
109-52-4
329 suppliers
$10.60/1gm:
![3,3-Dimethylacrylic acid](/CAS/GIF/541-47-9.gif)
541-47-9
348 suppliers
$5.00/10g
![Isovaleric acid](/CAS/GIF/503-74-2.gif)
503-74-2
401 suppliers
$5.00/10g
![3-Methyl-1-butanol](/CAS/GIF/123-51-3.gif)
123-51-3
519 suppliers
$25.00/25mL
![Isovaleric acid](/CAS/GIF/503-74-2.gif)
503-74-2
401 suppliers
$5.00/10g
![3-Methylbutyl 3-methylbutanoate](/CAS/GIF/659-70-1.gif)
659-70-1
324 suppliers
$7.00/25g