L-alpha-Cyclohexylglycine synthesis
- Product Name:L-alpha-Cyclohexylglycine
- CAS Number:14328-51-9
- Molecular formula:C8H15NO2
- Molecular Weight:157.21
103-01-5
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14328-51-9
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Yield:14328-51-9 94%
Reaction Conditions:
PtO2
Steps:
3.A (S)-2-Amino-2-cyclohexylacetic acid
EXAMPLE 3A (S)-2-Amino-2-cyclohexylacetic acid L-Phenylglycine (8.04 g, 53 mmol) was reduced by catalytic hydrogenation using PtO2 in 80% acetic acid (HOAc) (200 mL). The catalyst was removed by filtration and the HOAc removed under reduced pressure to afford the title compound as a white solid (7.8 g, 94%). The 300 MHz 1 H NMR spectrum was found to be consistent with the proposed structure. MS (FAB) m/e 158 (M+H)+.
References:
Abbott Laboratories US5338726, 1994, A
2935-35-5
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40651-95-4
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32908-36-4
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14328-51-9
256 suppliers
$6.00/5g