LAURYL LAURATE synthesis
- Product Name:LAURYL LAURATE
- CAS Number:13945-76-1
- Molecular formula:C24H48O2
- Molecular Weight:368.64
Yield: 98%
Reaction Conditions:
with high p-toluenesulfonate content diphenylamine and terephthalaldehyde resin in neat (no solvent) at 110; for 24 h;
Steps:
General Procedure for Transesterification Catalyzed by DTRT(H)
General procedure: A mixture of methyl 3-phenylpropionate (328 mg, 2.0 mmol), 1-octanol (390 mg, 3.0 mmol), and DTRT(H) (171 mg) was stirred at 110°C for 4 h. The mixture was treated in a manner similar to the procedure described above to give 11 (493 mg, 94%).
References:
Tanemura, Kiyoshi;Suzuki, Tsuneo [Organic Preparations and Procedures International,2016,vol. 48,# 1,p. 72 - 80]
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