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(+)-Lycoperdic acid synthesis

6synthesis methods
1-Oxa-7-azaspiro[4.4]nonane-7,8-dicarboxylic acid, 2,6-dioxo-, 7-(1,1-diMethylethyl) 8-Methyl ester, (5S,8S)-

146554-64-5
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(+)-Lycoperdic acid

69086-72-2
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-

Yield:69086-72-2 77%

Reaction Conditions:

with hydrogenchloride for 12 h;Heating;

References:

Kaname, Mamoru;Yoshifuji, Shigeyuki [Tetrahedron Letters,1992,vol. 33,# 52,p. 8103 - 8104]