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138302-49-5

Methyl 2-(dihydro-2H-pyran-4(3H)-ylidene)acetate synthesis

3synthesis methods
29943-42-8 Synthesis
Tetrahydro-4H-pyran-4-one

29943-42-8
426 suppliers
$5.00/1g

21204-67-1 Synthesis
methyl (triphenylphosphoranylidene)acetate

21204-67-1
17 suppliers
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Yield:138302-49-5 96.3%

Reaction Conditions:

with benzoic acid in toluene; for 8 h;Heating;Horner-Emmons condensation;

References:

Kuehne, Martin E;Bornmann, William G;Marko, Istvan;Qin, Yong;LeBoulluec, Karen L;Frasier, Deborah A;Xu, Feng;Mulamba, Tshilundu;Ensinger, Carol L;Borman, Linda S;Huot, Anne E;Exon, Christopher;Bizzarro, Fred T;Cheung, Julia B;Bane, Susan L [Organic and biomolecular chemistry,2003,vol. 1,# 12,p. 2120 - 2136]