![](/CAS/GIF/2965-22-2.gif)
METHYL 2-FLUORO-5-NITROBENZOATE synthesis
- Product Name:METHYL 2-FLUORO-5-NITROBENZOATE
- CAS Number:2965-22-2
- Molecular formula:C8H6FNO4
- Molecular Weight:199.14
![2-Fluoro-5-nitrobenzoic acid](/CAS/GIF/7304-32-7.gif)
7304-32-7
262 suppliers
$8.00/10g
![METHYL 2-FLUORO-5-NITROBENZOATE](/CAS/GIF/2965-22-2.gif)
2965-22-2
115 suppliers
$6.00/250mg
Yield: 210 mg (99%)
Reaction Conditions:
in hydrogenchloride;methanol
Steps:
77.A A.
A. Methyl 2-Fluoro-5-nitrobenzoate A solution of 2-fluoro-5-nitrobenzoic acid (200 mg, 1.08 mmol) in 0.7 M HCl in methanol was stirred for 5 h. The mixture was concentrated yielding 210 mg (99%) of the title compound; which was used without further purification.
References:
Eli Lilly and Company US6635657, 2003, B1
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
740 suppliers
$7.29/5ml-f
![2-Fluoro-5-nitrobenzoic acid](/CAS/GIF/7304-32-7.gif)
7304-32-7
262 suppliers
$8.00/10g
![METHYL 2-FLUORO-5-NITROBENZOATE](/CAS/GIF/2965-22-2.gif)
2965-22-2
115 suppliers
$6.00/250mg
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
740 suppliers
$7.29/5ml-f
![5-Amino-2-fluorobenzioc acid](/CAS/GIF/56741-33-4.gif)
56741-33-4
183 suppliers
$14.00/1g
![METHYL 2-FLUORO-5-NITROBENZOATE](/CAS/GIF/2965-22-2.gif)
2965-22-2
115 suppliers
$6.00/250mg
![Methyl 2-chloro-5-nitrobenzoate](/CAS/GIF/6307-82-0.gif)
6307-82-0
141 suppliers
$25.00/2.5g
![METHYL 2-FLUORO-5-NITROBENZOATE](/CAS/GIF/2965-22-2.gif)
2965-22-2
115 suppliers
$6.00/250mg
![2-Fluoro-5-nitrobenzoic acid](/CAS/GIF/7304-32-7.gif)
7304-32-7
262 suppliers
$8.00/10g
![Iodomethane](/CAS/GIF/74-88-4.gif)
74-88-4
340 suppliers
$15.00/10g
![METHYL 2-FLUORO-5-NITROBENZOATE](/CAS/GIF/2965-22-2.gif)
2965-22-2
115 suppliers
$6.00/250mg