methyl 3-(2-Pyridyl)propiolate synthesis
- Product Name:methyl 3-(2-Pyridyl)propiolate
- CAS Number:72764-93-3
- Molecular formula:C9H7NO2
- Molecular Weight:161.16
1945-84-2
227 suppliers
$12.00/1g
124-38-9
122 suppliers
$214.00/14L
74-88-4
342 suppliers
$15.00/10g
72764-93-3
31 suppliers
$45.00/50mg
Yield:72764-93-3 112.5 mg
Reaction Conditions:
Stage #1: 2-ethynylpyridine;carbon dioxidewith cesium fluoride;trimethylsilylacetylene in dimethyl sulfoxide at 30; for 20 h;
Stage #2: methyl iodide in dimethyl sulfoxide at 30; for 5 h;
References:
Yu;Yang;Gao;Yang;Zhao;Zhang;Liu [New Journal of Chemistry,2017,vol. 41,# 17,p. 9250 - 9255] Location in patent:supporting information
1945-84-2
227 suppliers
$12.00/1g
79-22-1
2 suppliers
$38.00/1000g
72764-93-3
31 suppliers
$45.00/50mg