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METHYL 3,4-DI-O-ACETYL-D-GLUCURONAL synthesis

4synthesis methods
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Yield:57690-62-7 62%

Reaction Conditions:

Stage #1: (2S,3S,4S,5R,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-carboxylic acid methyl esterwith hydrogen bromide;acetic acid
Stage #2: with zinc

References:

WO2008/138389,2008,A1 Location in patent:Page/Page column 5

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