Methyl 3,4-diaminobenzoate synthesis
- Product Name:Methyl 3,4-diaminobenzoate
- CAS Number:36692-49-6
- Molecular formula:C8H10N2O2
- Molecular Weight:166.18
67-56-1
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619-05-6
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36692-49-6
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$11.00/5g
Yield:36692-49-6 98.1%
Reaction Conditions:
with sulfuric acid at 90; for 12 h;Temperature;
Steps:
1.1; 2.1; 3.1; 4.1; 5.1; 6.1 (1)Synthesis of methyl 3,4-diaminobenzoate (2)
Take a 100 ml single-mouth bottle, add 3,4-diaminobenzoic acid (1) 3.04 g (0.02 mol), and add 50 mL of methanol.Stir and dissolve, then add 19.6 g (0.2 mol) of concentrated sulfuric acid.Stir at 90 ° C for 12 hours. After the reaction is completed,Methanol is distilled off under reduced pressure, and the residue is poured into ice water.Drying by suction filtration to obtain methyl 3,4-diaminobenzoate (2)3.26g,The yield was 98.1%.
References:
CN108997229,2018,A Location in patent:Paragraph 0015; 0025; 0028; 0031; 0034; 0037
99512-09-1
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36692-49-6
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36692-49-6
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619-05-6
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36692-49-6
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36692-49-6
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