METHYL 3-OXOHEPTANOATE synthesis
- Product Name:METHYL 3-OXOHEPTANOATE
- CAS Number:39815-78-6
- Molecular formula:C8H14O3
- Molecular Weight:158.2
638-29-9
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$14.14/1gm:
39815-78-6
114 suppliers
$91.67/25g
Yield: 79%
Reaction Conditions:
with calcium hydroxide in dichloromethane;butanone
Steps:
5 EXAMPLE 5
EXAMPLE 5 Under the same conditions as in Example 1, 116 g (1.0 mol) of methyl acetoacetate in a mixture of 520 ml of methylene chloride and 30 ml of methyl ethyl ketone were reacted with 77.8 g (1.05 mol) of calcium hydroxide and 138.7 g (1.15 mol) of valeryl chloride. The pH in this gave 151 g (GC purity 82.5%) of methyl valerylacetate (yield 79.0%).
References:
Wacker-Chemie GmbH US5194671, 1993, A
7732-18-5
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107-08-4
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105-45-3
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39815-78-6
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591-78-6
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616-38-6
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39815-78-6
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18937-78-5
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546-89-4
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39815-78-6
114 suppliers
$91.67/25g
67-56-1
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2033-24-1
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638-29-9
268 suppliers
$14.14/1gm:
39815-78-6
114 suppliers
$91.67/25g