![](/CAS/GIF/39815-78-6.gif)
METHYL 3-OXOHEPTANOATE synthesis
- Product Name:METHYL 3-OXOHEPTANOATE
- CAS Number:39815-78-6
- Molecular formula:C8H14O3
- Molecular Weight:158.2
![Valeryl chloride](/CAS/GIF/638-29-9.gif)
638-29-9
259 suppliers
$14.14/1gm:
![METHYL 3-OXOHEPTANOATE](/CAS/GIF/39815-78-6.gif)
39815-78-6
110 suppliers
$91.67/25g
Yield: 79%
Reaction Conditions:
with calcium hydroxide in dichloromethane;butanone
Steps:
5 EXAMPLE 5
EXAMPLE 5 Under the same conditions as in Example 1, 116 g (1.0 mol) of methyl acetoacetate in a mixture of 520 ml of methylene chloride and 30 ml of methyl ethyl ketone were reacted with 77.8 g (1.05 mol) of calcium hydroxide and 138.7 g (1.15 mol) of valeryl chloride. The pH in this gave 151 g (GC purity 82.5%) of methyl valerylacetate (yield 79.0%).
References:
Wacker-Chemie GmbH US5194671, 1993, A
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![METHYL 3-OXOHEPTANOATE](/CAS/GIF/39815-78-6.gif)
39815-78-6
110 suppliers
$91.67/25g
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![METHYL 3-OXOHEPTANOATE](/CAS/GIF/39815-78-6.gif)
39815-78-6
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$91.67/25g
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![METHYL 3-OXOHEPTANOATE](/CAS/GIF/39815-78-6.gif)
39815-78-6
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$91.67/25g
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![Valeryl chloride](/CAS/GIF/638-29-9.gif)
638-29-9
259 suppliers
$14.14/1gm:
![METHYL 3-OXOHEPTANOATE](/CAS/GIF/39815-78-6.gif)
39815-78-6
110 suppliers
$91.67/25g