Methyl-(4-Methyl-3-nitro-phenyl)-aMine synthesis

4synthesis methods

Product Name:Methyl-(4-Methyl-3-nitro-phenyl)-aMine
CAS Number:33992-16-4
Molecular formula:C8H10N2O2
Molecular Weight:166.1772

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33992-16-4
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Yield:33992-16-4 75%

Reaction Conditions:

Stage #1: 4,N,N-trimethyl-3-nitrobenzenaminewith 1,4-diaza-bicyclo[2.2.2]octane;rose bengal;acetic acid in acetonitrile at 20; for 6 h;Flow reactor;Irradiation;
Stage #2: with sulfuric acid in methanol;water at 20; for 12 h;

References:

Wu, Guolin;Li, Yazhen;Yu, Xuemei;Gao, Yu;Chen, Haijun [Advanced Synthesis and Catalysis,2017,vol. 359,# 4,p. 687 - 692] Location in patent:supporting information

119-32-4 Synthesis