METHYL N-BENZOYLANTHRANILATE synthesis

13synthesis methods

Product Name:METHYL N-BENZOYLANTHRANILATE
CAS Number:7510-49-8
Molecular formula:C15H13NO3
Molecular Weight:255.27

98-88-4 Synthesis

98-88-4
575 suppliers
$10.00/5g

134-20-3 Synthesis

134-20-3
580 suppliers
$16.00/25mL

7510-49-8
20 suppliers
$28.60/250mg

Yield:7510-49-8 97%

Reaction Conditions:

with pyridine in chloroform at 20;

Steps:

General procedure for the synthesis of compounds 24a-d and 25a,b.

General procedure: Solution of appropriate acyl chloride (2 mmol) in 15 ml CHCl₃ was added dropwise to a solution of compound 23a or 23b (2 mmol) and pyridine (2.5 mmol) in 15 ml CHCl₃. The reaction mixture was stirred overnight at r.t. Then it was washed with 5% HCl (3x10 ml), organic layer was dried over Na₂SO₄, solvent was removed under reduced pressure. The residue was chromatographed over SiO₂ with mixture of petroleum ether - ethyl acetate as eluent to give the products as a colorless solids. methyl 2-benzamidobenzoate (24a).3 Yield 97%.

References:

Piven, Yuri A.;Yastrebova, Margarita A.;Khamidullina, Alvina I.;Scherbakov, Alexander M.;Tatarskiy, Victor V.;Rusanova, Julia A.;Baranovsky, Alexander V.;Zinovich, Veronica G.;Khlebnicova, Tatyana S.;Lakhvich, Fedor A. [Bioorganic and Medicinal Chemistry,2022,vol. 53,art. no. 116521] Location in patent:supporting information

610-97-9 Synthesis