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ChemicalBook CAS DataBase List METHYLMERCURY(II) BROMIDE

METHYLMERCURY(II) BROMIDE synthesis

6synthesis methods
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Yield:506-83-2 30% ,612-00-0 35% ,91-01-0 47%

Reaction Conditions:

with potassium bromide in nitromethane;byproducts: N-(diphenylmethyl)acetamide; Ar atmosphere and absence of light and moisture; addn. of AgBF4 in nitromethane to soln. of alkylmercury, portionwise addn. of Ph2CHCl in nitromethane (20°C, TLC monitoring), washing with soln. of KBr; TLC;

References:

Uglova, E. V.;Petrovskii, K. B.;Fadeeva, S. S.;Mikhura, I. V.;Reutov, O. A. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1982,vol. 31,# 6,p. 1231 - 1234][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1982,# 6,p. 1382 - 1386]

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