Methyltetrazine-amine hydrochloride synthesis

3synthesis methods

Product Name:Methyltetrazine-amine hydrochloride
CAS Number:1596117-29-1
Molecular formula:C3H6ClN5
Molecular Weight:147.5662

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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: hydrazine; zinc trifluoromethanesulfonate / 80 °C / Inert atmosphere; Sealed tube
1.2: Inert atmosphere
2.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 2 h / 20 °C / Inert atmosphere

References:

Sarris, Alexi J. C.;Hansen, Thomas;de Geus, Mark A. R.;Maurits, Elmer;Doelman, Ward;Overkleeft, Herman S.;Codée, Jeroen D. C.;Filippov, Dmitri V.;van Kasteren, Sander I. [Chemistry - A European Journal,2018,vol. 24,# 68,p. 18075 - 18081]

tert-Butyl N-(((4-(6-methyl-1,2,4,5-tetrazin-3-yl)phenyl)methyl)carbamate

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References

15996-76-6 Synthesis

4-(Aminomethyl)benzonitrile hydrochloride

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References