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N-1-(pyrid-2-yl)propane-1,3-diamine synthesis

6synthesis methods
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Yield:38585-73-8 91%

Reaction Conditions:

with bis(1,5-cyclooctadiene)diiridium(I) dichloride;Py2NPiPr2;sodium t-butanolate in tetrahydrofuran;diethylene glycol dimethyl ether at 110; for 24 h;Inert atmosphere;chemoselective reaction;

References:

Blank, Benoit;Michlik, Stefan;Kempe, Rhett [Advanced Synthesis and Catalysis,2009,vol. 351,# 17,p. 2903 - 2911] Location in patent:experimental part