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ChemicalBook CAS DataBase List N-ACETYL SUCCINIMIDE
3027-06-3

N-ACETYL SUCCINIMIDE synthesis

6synthesis methods
-

Yield:3027-06-3 66%

Reaction Conditions:

with pyridine in dichloromethane; for 1 h;

Steps:

General procedure (II) for N-acylation of amines (preparation of authentic samples)

General procedure: To a stirred solution of the amine (2 g) in dichloromethane was added pyridine (1.2 eq.) followed by dropwise addition of the acid chloride(1.2 eq.). After 1 hr, further dichloromethane (10 ml) was added, the solution then washed successively with saturated aqueous sodium hydrogen carbonate, hydrochloric acid (2 M), water, then dried and the solvent removed under reduced pressure to give the amide.

References:

Al-Sehemi, Abdullah G.;Al-Amri, Reem S. Abdul-Aziz;Irfan, Ahmad [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2014,vol. 53,# 8,p. 1115 - 1121]

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