N-Benzyl-1-(thiophen-2-yl)MethanaMine synthesis

8synthesis methods

Product Name:N-Benzyl-1-(thiophen-2-yl)MethanaMine
CAS Number:73325-61-8
Molecular formula:C12H13NS
Molecular Weight:203.3033

98-03-3 Synthesis

98-03-3
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100-46-9 Synthesis

100-46-9
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73325-61-8
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Yield:73325-61-8 94%

Reaction Conditions:

with 1,4-diaza-bicyclo[2.2.2]octane;(2-chloro-6-fluorophenyl)bis(2,6-dichlorophenyl)borane;hydrogen in toluene at 80; under 15001.5 Torr; for 72 h;Glovebox;chemoselective reaction;

References:

Dorkó, éva;Szabó, Márk;Kótai, Bianka;Pápai, Imre;Domján, Attila;Soós, Tibor [Angewandte Chemie - International Edition,2017,vol. 56,# 32,p. 9512 - 9516][Angew. Chem.,2017,vol. 129,p. 9640 - 9644,5] Location in patent:supporting information