ChemicalBook CAS DataBase List N-Benzyloxycarbonyl-3-(4-chlorophenyl)-L-alanine

N-Benzyloxycarbonyl-3-(4-chlorophenyl)-L-alanine synthesis

5synthesis methods

Product Name:N-Benzyloxycarbonyl-3-(4-chlorophenyl)-L-alanine
CAS Number:127888-10-2
Molecular formula:C17H16ClNO4
Molecular Weight:333.77

7424-00-2 Synthesis

7424-00-2
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N-Benzyloxycarbonyl-3-(4-chlorophenyl)-L-alanine

127888-10-2
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: tetrahydrofuran / 50 °C
2.1: NMM / tetrahydrofuran / -25 - 20 °C
3.1: 10 mol percent (DHQD)2AQN; 4 Angstroem molecular sieves; methanol / diethyl ether / 18 h / -60 °C
3.2: 43 percent / H₂O

References:

Hang;Tian;Tang;Deng [Journal of the American Chemical Society,2001,vol. 123,# 50,p. 12696 - 12697]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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127888-10-2
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References

134306-44-8 Synthesis

Phenylalanine, 4-chloro-N-[(phenylmethoxy)carbonyl]-, methyl ester

134306-44-8
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127888-10-2
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References

13139-17-8
500 suppliers
$6.00/25g

127888-10-2
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References

14173-39-8
242 suppliers
$25.00/1G

501-53-1
397 suppliers
$10.00/1g

127888-10-2
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References

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