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ChemicalBook CAS DataBase List N-[BIS(METHYLTHIO)METHYLENE]GLYCINE METHYL ESTER
58091-08-0

N-[BIS(METHYLTHIO)METHYLENE]GLYCINE METHYL ESTER synthesis

3synthesis methods
-

Yield:58091-08-0 70%

Reaction Conditions:

Stage #1: carbon disulfide;methoxycarbonylmethylaminewith triethylamine in dichloromethane at 20; for 0.5 h;
Stage #2: methyl iodidewith triethylamine in dichloromethane;Heating;

References:

Krishnaswamy;Govande;Gumaste;Bhawal;Deshmukh [Tetrahedron,2002,vol. 58,# 11,p. 2215 - 2225]