N-HYDROXYBUTYRAMIDINE synthesis
- Product Name:N-HYDROXYBUTYRAMIDINE
- CAS Number:27620-10-6
- Molecular formula:C4H10N2O
- Molecular Weight:102.14
A solution of a mixture of butyronitrile, NaOH and hydroxylamine hydrochloride in 95% ethanol and water was refluxed Heat for 12 hours. The solvent was removed in vacuo, the oily residue was dissolved in chloroform , and insoluble NaCl was removed by filtration. The filtrate was concentrated in vacuo to give N-hydroxybutyramidine as a colorless oil.
109-74-0
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$20.00/25mL
27620-10-6
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$59.00/250mg
Yield:27620-10-6 72%
Reaction Conditions:
with hydroxylamine hydrochloride;sodium carbonate in ethanol;water at 55; for 0.5 h;Sonication;
References:
Barros, Carlos Jonnatan Pimentel;De Freitas, Jucleiton J. Rufino;De Oliveira, Ronaldo N.;De Freitas Filho, Jo?o R. [Journal of the Chilean Chemical Society,2011,vol. 56,# 2,p. 721 - 722] Location in patent:experimental part