![](/CAS/GIF/51285-13-3.gif)
N'-Hydroxycyclopropanecarboximidamide synthesis
- Product Name:N'-Hydroxycyclopropanecarboximidamide
- CAS Number:51285-13-3
- Molecular formula:C4H8N2O
- Molecular Weight:100.12
![Cyclopropanecarbonitrile](/CAS/GIF/5500-21-0.gif)
5500-21-0
304 suppliers
$16.00/5mL
![N'-Hydroxycyclopropanecarboximidamide](/CAS/GIF/51285-13-3.gif)
51285-13-3
112 suppliers
$12.00/100mg
Yield:51285-13-3 80%
Reaction Conditions:
with hydroxylamine;potassium carbonate in ethanol;water at 20; for 18 h;
Steps:
N-hydroxy-cyclopropanecarboxamidine
6.00 g (43.41 mmol) potassium carbonate are dissolved in 19 ml of water, 60 ml of ethanol, 3.00 g (43.17 mmol) hydroxylamine and 3.25 ml (43.25 mmol) cyclopropylcyamide are added. The reaction mixture is stirred for 18 hours at ambient temperature, then evaporated down and re-evaporated with toluene. The residue is mixed with ethanol, suction filtered and the filtrate is evaporated to dryness. Yield: 3.47 g (80% of theoretical)
References:
US2007/238730,2007,A1 Location in patent:Page/Page column 24