ChemicalBook CAS DataBase List N-Methyl-5-homopiperazinone

N-Methyl-5-homopiperazinone synthesis

1synthesis methods

Product Name:N-Methyl-5-homopiperazinone
CAS Number:60565-89-1
Molecular formula:C6H12N2O
Molecular Weight:128.17

N-(2-Cyanoethyl)-N-[(1,1-dimethylethoxy)carbonyl]glycine methyl ester

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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: hydrogen; platinum(IV) oxide / ethanol; chloroform / 16 h / 25 °C / 2585.81 Torr
2.1: sodium hydroxide / methanol / 2 h / 25 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 25 °C
3.2: 20 °C
4.1: trifluoroacetic acid / dichloromethane / 2 h / 25 °C

References:

US2015/197493,2015,A1

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