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ChemicalBook CAS DataBase List NAPHTHALENE-1-D1

NAPHTHALENE-1-D1 synthesis

11synthesis methods
-

Yield:875-62-7 99%

Reaction Conditions:

Stage #1: 1-Fluoronaphthalenewith C78H70Al2Cl4N6P4Rh2;magnesium;ethylene dibromide in tetrahydrofuran at 20; for 22 h;Inert atmosphere;Glovebox;
Stage #2: with water-d2 in tetrahydrofuran;

References:

Fujii, Ikuya;Semba, Kazuhiko;Li, Qiao-Zhi;Sakaki, Shigeyoshi;Nakao, Yoshiaki [Journal of the American Chemical Society,2020,vol. 142,# 27,p. 11647 - 11652] Location in patent:supporting information

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