-NETA synthesis
- Product Name:-NETA
- CAS Number:115066-04-1
- Molecular formula:C16H20INO
- Molecular Weight:369.25
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Yield:115066-04-1 58%
Reaction Conditions:
in ethanol at 20; for 24 h;
Steps:
1 General Synthesis of Quaternary Ammonium Salts 22-33:
General procedure: The tertiary amine 21 (Table 3, 1.0 eq, 1.0 mmol) was suspended in ethanol (5 mL) in a 14 mL glass vial then methyl iodide (1.2 eq, 1.2 mmol) was added dropwise at ambient temperature and stirred for 24 h, during which time the a white solid precipitated. The solid was collected by filtration and washed with copious amounts of ethanol followed by diethyl ether. The compounds were further purified by stirring them in mixture of acetonitrile and diethyl ether for overnight. The desired compounds were obtained as off-white to pale brown solids.
References:
US2020/345661,2020,A1 Location in patent:Paragraph 0200; 0250-0251; 0252
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