NIOBIUM(III) BROMIDE ETHYLENE GLYCOL synthesis
- Product Name:NIOBIUM(III) BROMIDE ETHYLENE GLYCOL
- CAS Number:126083-88-3
- Molecular formula:C4H13Br3NbO2
- Molecular Weight:425.76
110-71-4
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Yield:126083-88-3 88%
Reaction Conditions:
in neat (no solvent);N2 atmosphere; addn. of NbBr5 to mixt of dimethoxyethane and (Bu)3SnH (-78°C, stirring), stirring (3.5 h), warming to room temp. (1 h); filtration, washing (dimethoxyethane, pentane), drying (vac.); elem. anal.;
References:
Hartung Jr., Jack B.;Pedersen, Steven F. [Organometallics,1990,vol. 9,# 5,p. 1414 - 1417]