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ChemicalBook CAS DataBase List Obeticholic Acid Impurity 13
1537866-49-1

Obeticholic Acid Impurity 13 synthesis

1synthesis methods
951694-73-8 Synthesis
(R)-methyl 4-((3R,5S,6R,7R,10S,13R)-6-ethyl-3,7-dihydroxy-10,13-dimethyl-hexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoate

951694-73-8
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Obeticholic Acid Impurity 13

1537866-49-1
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Yield:-

Reaction Conditions:

with methanol;lithium borohydride in tetrahydrofuran at 0;

References:

D'Amore, Claudio;Di Leva, Francesco Saverio;Sepe, Valentina;Renga, Barbara;Del Gaudio, Chiara;D'Auria, Maria Valeria;Zampella, Angela;Fiorucci, Stefano;Limongelli, Vittorio [Journal of Medicinal Chemistry,2014,vol. 57,# 3,p. 937 - 954]

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