Octafluoronaphthalene synthesis
- Product Name:Octafluoronaphthalene
- CAS Number:313-72-4
- Molecular formula:C10F8
- Molecular Weight:272.09
2234-13-1
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$21.00/1g
313-72-4
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$10.00/250mg
Yield:313-72-4 85%
Reaction Conditions:
with sulfolane;potassium fluoride at 130 - 250; for 5 h;
Steps:
1 Example 1: Step (1) Fluorine reaction
120 g of octachloronaphthalene and 500 g of sulfolane were placed in a three-necked flask, and 210 g of potassium fluoride was quickly added under stirring, and heated to 250 ° C for 5 hours.The reaction was completed, the temperature was lowered to 130 ° C, and distillation under reduced pressure gave 68.8 g of octafluoronaphthalene solid. The yield of this step was 85%.
References:
CN108101729,2018,A Location in patent:Paragraph 0012
306-94-5
212 suppliers
$9.00/5G
313-72-4
213 suppliers
$10.00/250mg
