ChemicalBook CAS DataBase List p-Aminobenzamide

p-Aminobenzamide synthesis

14synthesis methods

Product Name:p-Aminobenzamide
CAS Number:2835-68-9
Molecular formula:C7H8N2O
Molecular Weight:136.15

873-74-5
628 suppliers
$9.00/1g

2835-68-9
439 suppliers
$5.00/5g

Yield:2835-68-9 100%

Reaction Conditions:

with C₁₈H₅₇O₃P₆Ru₂⁽¹⁺⁾*C₆H₅O^(1-)*C₆H₆O;water in 1,4-dioxane; for 48 h;Sealed tube;Inert atmosphere;Schlenk technique;Time;

Steps:

(B):

General procedure: Complex 3 (18.3 mg, 0.0204 mmol), 1,4-dioxane (1.0 ml),benzonitrile (103.7 mg, 1.18 mmol), water (100 μl, 5.53 mmol)were added in a screw-cap tube. The reaction mixture was heatedat 100 °C for 12 h. After cooling the reaction mixture to room temperature,dibenzyl and methanol (1 ml) were added to give ahomogeneous solution and the products were analyzed by GLC.

References:

Kiyota, Sayori;Kobori, Takako;Soeta, Hirofumi;Ichikawa, You-ichi;Komine, Nobuyuki;Komiya, Sanshiro;Hirano, Masafumi [Polyhedron,2016,vol. 120,p. 3 - 10]