![](/CAS/GIF/7472-54-0.gif)
P-BENZANISIDIDE synthesis
- Product Name:P-BENZANISIDIDE
- CAS Number:7472-54-0
- Molecular formula:C14H13NO2
- Molecular Weight:227.26
![Iodobenzene](/CAS/GIF/591-50-4.gif)
591-50-4
472 suppliers
$10.00/1g
201230-82-2
1 suppliers
inquiry
![p-Anisidine](/CAS/GIF/104-94-9.gif)
104-94-9
475 suppliers
$9.00/1g
![P-BENZANISIDIDE](/CAS/GIF/7472-54-0.gif)
7472-54-0
60 suppliers
$12.00/1mg
Yield:7472-54-0 100%
Reaction Conditions:
with triethylamine in N,N-dimethyl-formamide at 100; under 750.075 Torr; for 8 h;Schlenk technique;Inert atmosphere;
Steps:
2.3.2. Catalytic reactions at atmospheric pressure
General procedure: In a typical experiment a solution containing the palladiumcatalyst (with 6 mol Pd-content) was placed in a Schlenk-tube.Under argon, 0.2 mmol (22.5 l) iodobenzene (1), 0.5 mmol aminereagent, 0.7 mmol (100 l) triethylamine and 1 ml solvent wasadded and the atmosphere was changed to carbon monoxide. Thereaction mixture was heated with stirring in an oil bath at 100Cand was analysed by gas chromatography.
References:
Urbán, Béla;Papp, Máté;Srankó, Dávid;Skoda-F?ldes, Rita [Journal of Molecular Catalysis A: Chemical,2015,vol. 397,p. 150 - 157]
![Benzaldehyde](/CAS/GIF/100-52-7.gif)
100-52-7
944 suppliers
$20.37/250g
![p-Anisidine](/CAS/GIF/104-94-9.gif)
104-94-9
475 suppliers
$9.00/1g
![P-BENZANISIDIDE](/CAS/GIF/7472-54-0.gif)
7472-54-0
60 suppliers
$12.00/1mg