P-BROMO-N-CYCLOHEXYL-N-METHYLANILINE synthesis

5synthesis methods

Product Name:P-BROMO-N-CYCLOHEXYL-N-METHYLANILINE
CAS Number:88799-11-5
Molecular formula:C13H18BrN
Molecular Weight:268.19

62-53-3 Synthesis

62-53-3
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: acetic acid; sodium cyanoborohydride / tetrahydrofuran / 18 h / 23 - 50 °C / Inert atmosphere
2.1: acetic acid; sodium cyanoborohydride / tetrahydrofuran / 18 h / 23 - 50 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 23 °C / Inert atmosphere
4.1: sulfurous dibromide / tetrahydrofuran / 4 h / -78 °C / Inert atmosphere
4.2: 0.75 h / -78 - 23 °C / Inert atmosphere

References:

Reed, Hayley;Paul, Tyler R.;Chain, William J. [Journal of Organic Chemistry,2018,vol. 83,# 18,p. 11359 - 11368]

108-94-1 Synthesis