![](/CAS/GIF/76-01-7.gif)
PENTACHLOROETHANE synthesis
- Product Name:PENTACHLOROETHANE
- CAS Number:76-01-7
- Molecular formula:C2HCl5
- Molecular Weight:202.29
![Trichloroethylene](/CAS/GIF/79-01-6.gif)
79-01-6
439 suppliers
$17.60/100ml
![PENTACHLOROETHANE](/CAS/GIF/76-01-7.gif)
76-01-7
56 suppliers
$38.39/5ml-a
Yield:76-01-7 99%
Reaction Conditions:
with chlorine at 10 - 20; for 11 h;Inert atmosphere;Cooling with ice;
Steps:
1 [Example 1] First step (TCE → C2Cl5H)
In a 500 mL glass three-necked flask, 500 g (3.8 mol) of TCE was weighed. After replacing the inside of the system with nitrogen, the reaction solution was cooled by an ice bath. Then, Cl2 was introduced at 180 mL / min under stirring. After introducing 1.0 equivalent (270 g, 3.8 mol) of Cl2, Nitrogen was introduced to expel Cl2 remaining in the system. As a result, 723 g (yield 99%) of the target pentachloroethane was obtained as a colorless transparent liquid with a GC purity of 97.9%.
References:
JP2021/20870, 2021, A Location in patent:Paragraph 0015-0016
![1,1-Dichloroethane](/CAS/GIF/75-34-3.gif)
75-34-3
97 suppliers
$22.69/48602
![1,1,2-Trichloroethane](/CAS/GIF/79-00-5.gif)
79-00-5
194 suppliers
$15.00/10 mL
![PENTACHLOROETHANE](/CAS/GIF/76-01-7.gif)
76-01-7
56 suppliers
$38.39/5ml-a
![1,1,2,2-Tetrachloroethane](/CAS/GIF/79-34-5.gif)
79-34-5
246 suppliers
$10.00/5g
![1,1-Dichloroethane](/CAS/GIF/75-34-3.gif)
75-34-3
97 suppliers
$22.69/48602
![1,1,2-Trichloroethane](/CAS/GIF/79-00-5.gif)
79-00-5
194 suppliers
$15.00/10 mL
![1,1,1,2-TETRACHLOROETHANE](/CAS/GIF/630-20-6.gif)
630-20-6
85 suppliers
$44.60/40335
![PENTACHLOROETHANE](/CAS/GIF/76-01-7.gif)
76-01-7
56 suppliers
$38.39/5ml-a
![1,1,2,2-Tetrachloroethane](/CAS/GIF/79-34-5.gif)
79-34-5
246 suppliers
$10.00/5g
![1,1-Dichloroethane](/CAS/GIF/75-34-3.gif)
75-34-3
97 suppliers
$22.69/48602
![1,1,2-Trichloroethane](/CAS/GIF/79-00-5.gif)
79-00-5
194 suppliers
$15.00/10 mL
![PENTACHLOROETHANE](/CAS/GIF/76-01-7.gif)
76-01-7
56 suppliers
$38.39/5ml-a
![Hexachloroethane](/CAS/GIF/67-72-1.gif)
67-72-1
268 suppliers
$11.00/25g
![1,1,2,2-Tetrachloroethane](/CAS/GIF/79-34-5.gif)
79-34-5
246 suppliers
$10.00/5g
![Hexachloroethane](/CAS/GIF/67-72-1.gif)
67-72-1
268 suppliers
$11.00/25g
![Glycerol](/CAS/GIF/56-81-5.gif)
56-81-5
1635 suppliers
$5.00/25g
![Tetrachloroethylene](/CAS/GIF/127-18-4.gif)
127-18-4
721 suppliers
$14.80/1ml
![2,3-DICHLORO-1-PROPANOL](/CAS/GIF/616-23-9.gif)
616-23-9
137 suppliers
$39.50/5g
![1,3-Dichloro-2-propanol](/CAS/GIF/96-23-1.gif)
96-23-1
281 suppliers
$10.00/1g
![PENTACHLOROETHANE](/CAS/GIF/76-01-7.gif)
76-01-7
56 suppliers
$38.39/5ml-a